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  • X-Ray Diffractometer(XRD)
X-Ray Diffractometer(XRD)

X-Ray Diffractometer(XRD)

  • Model: PDW-XRD-2700A
  • Product description: X-Ray Diffractometer(XRD)
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1Applications

It can accurately measure metal and non-metal samples, do qualitative and quantitative analysis. When it is work with the corresponding accessories, it also can be used to analysis the influence of high temperature and low temperature on the material structure and analysis the structure of the film sample, metal material texture, stress measurement, etc.

 

2Functions

This XRD adopts the most advanced technology. The angle accuracy and precision of the goniometer has reached world advanced l
evel.  The x ray source and detector can work stably   for a long time to ensure the accuracy and precision of diffraction peak position, peak shape and intensity measurement. Powder phase analysis, grain size judgment, crystalline analysis, phase content analysis, film analysis, small Angle particle size analysis. This XRD include high stability X-ray generator, high precision goniometer, closed proportional detector, data processing software, related application software, etc.

 

3Characteristics

 

lHigh stability X-ray source: the XRD adopts AF3 model high frequency &high voltage X-ray generator, greatly improving the stability of the XRD measurement results;

 

lLong life X-ray tube: metal-ceramic X-ray tube has the characteristics of good heat dissipation, high running power (40kV ×40mA) and long service life;

 

lHigh precision goniometer: the diffraction angle drive adopts servo motor drive +  optical coding control technology, with accurate positioning and high measurement accuracy; The hidden design of the goniometer makes the performance of the instrument more neat, beautiful and generous. Within the scope of the diffraction angle measurement, the diffraction angle is less than 0.02 ° linearity;

 

lIt can work with temperature attachment, multifunctional sample holder and other XRD accessories friendly, it can "plug and play". The software automatic identification control technology, convenient for the use of the instrument operators.

 

lX-ray protection is safe and reliable: X-ray scatterer protection device is safe and reliable, the X-ray protection door is automatically forbidden to open when XRD is measuring sample, double protection can prevent the operator from being exposed to scattering radiation under any circumstances.

 

4Main Technical parameters
4.1 High stability X-ray source Unit AF3 model High Frequency &High Voltage X-ray generator

lRated power3 kW (HF,HV control technology)

lTube voltage10~60kV, 1kV/step;

lTube current5~50mA, 1mA/step;

lStability of tube voltage and tube current≤0.005% ;

lThere is Protection for over voltage, over current and over power and water depletion.

lX-ray tubemetal ceramic x-ray tube / Cu Target / Focus size: 1×10mm²/ 2.4kW .

 

4.2 High Precision Goniometer Unit

lGoniometerAdopt servo motor and optical coding technique to drive θs and θd;

lScanning modeθ—θ goniometer; it is vertical; the sample is put horizontally ;

l2θmeasuring range-6°~160°; Radius of goniometer: 225mm;

lScanning mode: continuous, stepping and Omg;

lMinimum step width Angle0.0001˚;

lAngle accuracy≤0.001˚; Angle repeatability≤0.0001˚ .

lIt can cancel the idle running and do angle calibration automatically.

lAngle locating speed1500˚/min;

lDiffraction Angle linearity: the Angle deviation of all peaks within the  full spectrum shall not exceed ±0.02°.

4.3 Detector Unit

 

Closed proportional Detector

lSpectral resolution: 25% Cu Kαspectral line;

lMaximum linear count rate: 5×105cps

 

4.4 Protection

 

X -ray scattering ray protection device is safe and reliable with interlocking mechanism. When the sample is measured, the radiation-shielding door is automatically forbidden to open, which can protect the operator from the scattering ray radiation under any circumstances, and the scattering ray dose conforms to the international standard 1.0 sv/h.

 

4.5 Control and processing software

lWindows 10 operating system;

lQualitative and quantitative analysis of material phases , Kα1 ,α2 peeling, Full spectrum fitting, peak fitting, FWHM and grain size calculation, crystal cell measuring, second
 

kind stress calculation, diffraction line indexation, multiple plotting, 3D plotting, diffraction data calibration, background subtraction,

quantitative analysis without standards, full spectral image fitting (WPF), XRD diffraction image simulation, etc.

5Working condition

lEnvironment temperature:20±5℃;

lRelative Humidity:30% ~ 80%;

lPower supply:3 phases,380V,50 Hz (If user′s is different, please inform),single phase power≥30 a

lGround resistance≤4Ω;

lThere should be no high frequency and arc interference caused by the tool, welding machine, high frequency furnace and other equipment.

lCooling water quality shall meet the requirements of X-ray tube;

lThe surrounding environment should not be flammable, corrosive gases, dust and vibration.

 

6AL-2700A XRD Configuration List

Part

Element Name

Unit

Qty

Remark

 

 

 

X-ray high-voltage generator

 AF3 X-ray high-frequency high-voltage generator

Set

1

Solid technology

X27.05 high voltage cable100kVP

Piece

1

Length3.0 meter

③3310 pipe sleeve

set

1

including automatic optical shutter

 X25.07 X-ray generator auto control system

set

1

Including 1 piece power cable

X25.02 stageMetal shell

set

1

Lead+ lead glass protection

 AS2901/24 Metal ceramic insulation X-ray tube

Piece

1

Cu target, 2.4kW

 

 

 

 

 

Goniometer System

①AG-3512H/AL-2700A goniometer

set

1

θ-θ

② Slit and powder sample holder

set

1

1 set for each

③ Through-hole sample plate

Piece

5

Aluminium matrix

④ Blind-hole sample plate

Piece

15

Quartz matrix

⑤ Filter

Piece

1

Match with target material

 Slit Plate and Lighting System Adjustment Accessories

 

set

 

1

 

 

Recording and controlling system

①Closed proportional detector

set

1

Including connecting cable

②Recording and controlling unit

set

1

 

③Motor and communication cable

set

1

2 motor cables, 1 communication cable

④Power supply unit

set

1

 

Circulating water cooling system

①ALC-3 Circulating water cooling system

set

1

Split structure

②Circulating water connecting tube

Piece

2

 

 

PC system

① CPU: Intel i series; RAM: 4G; Hard drive: 128G; 19 inch LED; GPU: high performance HD series.

 

set

 

1

 

DELL

② A4 laser printer

set

1

HP1108

 

 

System Control and Applicable Software

 AL Series Diffractometer Control Program Software

set

1

Windows10

② Phase qualitative and quantitative analysis software

 

set

 

1

 

③Data processing and application software

set

1

Jade 6

④Diffraction data card base

set

1

PDF2

⑤Crystal Structure Data Base

set

1

ICSD

 

 

Technical documents

 AL series XRD user manual

Copy

1

 

②Data Process and Application Software User Manual

 

Copy

 

1

 

③ALC-3 Circulating Water Cooling System User Manual

 

Copy

 

1

 

Accessary

①ALS-3 crystal graphite monochromator

set

1

Reflectivity28%

 

Spare parts

Fuses 11.522.533+A

Piece

10

10 pieces for each

②Tools

set

1

 

③Agate Mortar ф100mm

set

1

 


7Packing information (for reference only)

Host package1190*1020*2000mm(L*W*H)
Gross Weight ≈350KG
Accessaries package1250*1035*1050mm (L*W*H)
Gross Weight ≈240KG

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