It is designed for commercial process and quality control. It is a concentration of advanced technology of XRD production, with multi-function and miniaturization. It can do qualitative analysis, quantitative analysis and crystal structure analysis on metal and nonmetal sample, especially for catalyst, titanium dioxide, cement and pharmacy industries.
Equipment Performance
●High frequency high voltage X-ray generator has greater stability, so it guarantees the repeatability of the data.
●Goniometer θs, θd arm adopts servo motor drive and optical encoder control technology, so the goniometer rotates more smoothly, the diffraction angle measuring is more accurate and the linearity is
better. Within the diffraction angle range, the diffraction linearity <0.02.
●The scattered ray protective device is safer and more reliable. When it is measuring samples, the protective door will be auto-locked to avoid the radiation to the people.
●DW-XRD-27mini XRD adopts the most advanced metal ceramic X-ray tube, it has long service life (3000 hours); the automatic 6-sample changer can improve the sample measuring speed and convenient for the operator.
●The compact structure can installed onto the platform without special laboratory environment. It is easy for operation and maintenance.
Application
ADW-XRD-27mini XRD can do qualitative and quantitative analysis on polycrystalline material. During qualitative analysis, it will indentify the unknown structure by comparing the measuring data with known phase data base. During quantitative analysis, it can describe the characteristics of the solid mixture, so that to confirm relative content of the crystalline compounds or un-crystallized phase.
Technical parameters
Service rating (Tube voltage, tube current) |
600W(40kV,15mA) or 1200W(40kV,30mA),Stability:0.005% |
|
X-ray tube |
Metal-ceramic X-ray tube, Cu target, Power 2.4kW, Focus size: 1 x 10 mm,Air cooling or water cooling(water flow rate >1L/min) |
|
Goniometer |
θs-θd , diffraction radius 150mm |
|
Measuring method |
Continuous, stepping, Omg |
|
Angular measurement range |
Druing leakage time, θs/θd is -3°~150°. |
|
Minimum step width |
0.0001° |
|
Angular reproducibility |
0.0001° |
|
Drive mode |
servo motor drive + optical encoder control technology |
|
Angle Positioning speed |
1500°/min |
|
Counter |
Closed Proportional detector or High speed one-dimensional semiconductor counter |
|
Energy spectrum resolution |
<25% |
|
Max. linear counting rate |
≥5×105cps(Proportional),≥1×107cps(One-dimensional semiconductor) |
|
Computer |
Dell laptop |
|
Software |
Controlling software |
Windows 7 operating system; control the tube voltage, tube current, shutter of the X-ray generator and do aging training automatically; Control the goniometer continuous or stepping scanning and diffraction data collection; do routine processing: automatic peak-seeking, manual peaking-seeking, integrated intensity, peak height, core, background deduction, smoothness, Peak shape amplification and spectrogram comparation, etc. |
Data processing software |
Qualitative and quantitative analysis of material phases , Kα1 ,α2 peeling, Full spectrum fitting, peak fitting, half-width and grain size calculation, crystal cell measuring, second kind stress calculation, diffraction line indexation, multiple plotting, 3D plotting, diffraction data calibration, background subtraction, quantitative analysis without standards, full spectral image fitting (WPF), XRD diffraction image simulation, etc. |
|
Scattered radiation protection |
Lead+ lead glass protection, shutter windows and protective guard linkage, the scattered radiation dose not exceeding 1μSv/h. |
|
Instrument Comprehensive regulation |
≤1‰ |
|
Sample quantity of one-time loading |
Auto sample changer, 6 samples can be put one time. |
|
Overall dimension |
600×410×670(w×d×h)mm |
DW-XRD-27 MINI Desktop XRD Configuration Table
Name |
Components |
Unit |
Qt |
y Remark |
X-ray high-voltage generator |
XRD40*600 X-ray generator |
set |
1 |
high-frequency high-voltage |
X27.06 high-voltage cable(75kVP) |
piece |
1 |
Length:2.0 meter |
|
3311 pipe sleeve (including automatic optical shutter) |
set |
1 |
|
|
X25.02 stage(Metal shell) |
set |
1 |
Lead+ lead glass protection |
|
DS2910/24 Metal ceramic insulation X-ray tube |
piece |
1 |
Cu target, 2.4kW |
|
Angle measurement system |
DG-3511 goniometer |
set |
1 |
θ-θ structure |
Slit and powder sample holder |
set |
1 |
One set for each |
|
Through-hole sample plate |
piece |
5 |
Aluminium matrix |
|
Blind-hole sample plate |
piece |
10 |
Glass matrix |
|
Filter |
piece |
1 |
Match with target material |
|
Slit plate and lighting system adjustment accessories |
set |
1 |
|
|
Recording and controlling system |
Closed proportional counter |
set |
1 |
Including 1 piece of connecting cable |
Recording and controlling unit |
set |
1 |
|
|
Motor and communication cable |
piece |
1 |
2 motor cables, 1 communication cable |
|
Power supply unit |
set |
1 |
|
|
PC system |
Dell laptop; I3 processor; RAM:4G; Hard drive: 500G; |
set |
1 |
DELL |
A4 laser printer |
set |
1 |
|
|
|
AL Series Diffractometer Control Program Software |
set |
1 |
Windows OS |
Diffraction data processing software |
set |
1 |
|
|
Diffraction data card base |
set |
1 |
2009 version(59) |
|
Crystal Structure Data Base |
set |
1 |
2010 version |
|
Technical documents |
AL series XRD user manual |
copy |
1 |
|
Data Process and Applicable Software User Manual |
copy |
1 |
|
|
Accessory |
DCX-6 sample changer |
set |
1 |
|
Graphite monochromator |
set |
1 |
Reflectivity>28% |
|
Spare parts |
Fuses 1、1.5、2、2.5、3、3+(A) |
Piece |
10 |
10 pieces for each |
Tools |
set |
1 |
|
|
Agate Mortar ф100mm |
set |
1 |
|